Nashrieh Shimi va Mohandesi Shimi Iran

Nashrieh Shimi va Mohandesi Shimi Iran

Sonochemical Syntheses of a Nano Copper (II) Coordination Compounds and Investigation of Their Conversion to Copper Oxide Nano Particles

Document Type : Research Article

Authors
Sara Chamani Goran
Gholam Hossein Shahverdizadeh
Department of Chemistry, Tabriz Branch, Islamic Azad University, Tabriz, I.R. IRAN
Abstract
Nano-structure of new Cu(II) coordination compound,[Cu(DPC)(H2O)3] was synthesized by sonochemical method. The new nano-structure was characterized by scanning electron microscopy(SEM), X-Ray powder Diffraction (XRD), IR spectroscopy, elemental analyses, and UV-Vis spectroscopy. The thermal stability of the compound has been studied by thermal gravimetric and differential thermal analyses. Copper oxide nanoparticles were obtained by direct calcination of the compound at 450, 500,550, and 600 under air atmospheres have different morphologies of nano-sized CuO. Also, the Nanoparticle of CuO was obtained by thermolysis of nano complexes in 180 with oleic acid as surfactant.
Keywords
Sonochemical
Nanoparticles
Surfactant
Copper(II) oxide

Subjects

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